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The dual HPLC and mass-spec approach is the correct standard, since purity and identity are separate questions and a compound can be pure yet incorrectly identified

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These were later named the Galilean moons in his honor

Both bile and pancreatic juice inhibit copper absorption in experimental work, but studies using radioisotopes did not show any difference in copper absorption by healthy volunteers, patients with untreated chronic pancreatitis or those on pancreatic extracts (H Sharma, P Tasker, JM Braganza, unpublished)